A high throughput screening hplc-fld method for paralytic shellfish toxins (psts) enabling effective official control

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  • who: Melania Siracusa et al. from the Batch-to-batch method performances and results reliability are guaranteed by strict quality control (QC)One surely blank and one fortified sample (QC+) are processed in each analytical batch. Repeatability is measured in every single batch by multiple injections of the MSd. Furthermore, the recovery factor is calculated in each batch. Control charts are built to monitor the batch-to-batch results, charts (Shewhart chart) are compiled with spiked sample recoveries, and, Charts are built to measure the repeatability of double-analyzed spiked bivalve samples. The here described PSTs analytical . . .

     

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