HIGHLIGHTS
- who: Santiago Rodru00edguez-Jimu00e9nez and colleagues from the MaterialsAll synthetic procedures involving air- or moisturesensitive materials were carried out under an inert , atmosphere by using Schlenk techniques. Solvents were purchased dried (e_g, DMF) or dried using standard purification procedures under an inert atmosphere. Reagents for synthesis were purchased from commercial suppliers in the highest purity available and used without further purification. , and , gas bottles (2% methane internal standard) were purchased from BOC. Na, (99%), [Co(H O)6](BF4), (>99%), (+)-sodium, ascorbate (>99%), iodomethane (99%), sodium acetate (99%), tetrabutylammonium hexafluorophosphate (TBAPF6, >99%), , u2032-dimethyl-2, u2032-dipyridyl . . .
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